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    电感耦合等离子体质谱法测定野波罗蜜根皮中9种微量元素

    Determination of 9 Trace Elements in Wild Jackfruit Root Bark by ICP-MS

    • 摘要: 采用电感耦合等离子体质谱法测定野波罗蜜根皮中9种微量元素。样品经煎煮法提取,提取液采用D101大孔树脂柱分离净化后测定。9种元素的总提取率在0~55.4%之间,浸留比为0~125%,颗粒吸附率在0~3.1%之间。9种元素的线性范围均在200 μg·L-1以内,检出限(3σ)在3.61~68.00 ng·L-1之间。按试验方法对标准样品进行分析,测定值与认定值相符,测定值的相对标准偏差(n=5)不大于2.4%。

       

      Abstract: ICP-MS was applied for the determination of 9 trace elements in wild jackfruit root bark. The sample was extracted by boiling method and the extract was purified with D101 macro-porous adsorption resin for detection. The extractive rates of the 9 elements were in the range of 0-55.4%. The immerse-residue ratios were in the range of 0-125%. The adsorption ratios were between 0-3.1%. The linear ranges of the 9 elements were within 200 μg·L-1, detection limits were in the range of 3.61-68.00 ng·L-1. The standard sample was analyed by the proposed method, the results obtained were in consistency with the certified values, measurements of RSD (n=5) was not more than 2.4%.

       

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