高级检索

    气相色谱法测定木制食品接触材料中游离甲醛

    GC Determination of Free Formaldehyde in Wooden Food Contacting Materials

    • 摘要: 提出了气相色谱法测定食品接触材料木制品中游离甲醛含量的方法。样品经水提取,所得提取液用2,4-二硝基苯肼衍生化,产物经环己烷萃取,用SPB-5型色谱柱(15 m×0.32 mm,0.25 μm)分离,以电子捕获检测器测定。方法的检出限(3S/N)为0.50 mg·kg-1。在3个标准加入水平下进行了回收率和精密度试验,测得回收率在72%~110%之间,测定值的相对标准偏差(n=6)在6.4%~13%之间。

       

      Abstract: A method of GC was applied to the determination of free formaldehyde in wooden food contacting materials. Sample was extracted with water, the extract obtained was derivitized with 2,4-dinitrophenyldrazine. The derivate was extracted with n-hexane and used for GC analysis. The SPB-5 column (15 m×0.32 mm, 0.25 μm) was used for separation, and electron capture detector was used for determination. Value of limit of detection (3S/N) found was 0.50 mg·kg-1. Tests for recovery and precision were made by standard addition method at 3 concentration levels, values of recovery and RSD′s (n=6) found were in the ranges of 72%-110% and 6.4%-13%.

       

    /

    返回文章
    返回