Abstract: The sample of toy materials was treated by microwave assisted digestion,and the contents of Al,Sb,As,Ba,B,Cd,Cr,Co,Cu,Pb,Mn, Hg,Ni,Se,Sr,Sn and Zn in the sample solution were determined by ICP-MS.The polyatomic ion effect was eliminated by collision cell technique (CCT).The values of detection limit of the method found were in the range of 0.003-0.09 μg·L-1.The proposed method was applied in the analysis of sample of colorized cloth,giving values of recovery in the range of 84.5%-106.0%,and RSD′s (n=7) in the range of 1.00%-5.79%.This method has favorably met with the testing requirements of EU directives for toy materials.