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    ZHOU Yun-long, DING Yin-xiang, HU Zhi-biao, YUAN Qiu-lan, TUO Hong-gui. Linear Scanning Polarographic Determination of Raceanisodamine[J]. PHYSICAL TESTING AND CHEMICAL ANALYSIS PART B:CHEMICAL ANALYSIS, 2011, 47(4): 422-423.
    Citation: ZHOU Yun-long, DING Yin-xiang, HU Zhi-biao, YUAN Qiu-lan, TUO Hong-gui. Linear Scanning Polarographic Determination of Raceanisodamine[J]. PHYSICAL TESTING AND CHEMICAL ANALYSIS PART B:CHEMICAL ANALYSIS, 2011, 47(4): 422-423.

    Linear Scanning Polarographic Determination of Raceanisodamine

    • Electrochemical behavior of receanisodamine was studied by linear scanning polarography and cyclic voltammetry. In a PBS of pH 6.70, a sensitive adsorptive wave of Raceanisodamine was observed at the potential of -1.095 V (vs. SCE). Linear relationship between values of 1st derivative peak current and concentration of raceanisodamine was kept in the range of 0.10-10.0 mg·L-1, with its detection limit (3S/N) of 0.06 mg·L-1. Precision was tested at the concentration level of 5.0 mg·L-1, value of RSD (n=6) found was 0.34%. The method was used in the analysis of raceanisodamine tablets, giving results in consistency with the labelled value.
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