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熊相群:气相色谱-质谱法快速测定水中6种有机磷农药的残留量


              7. 1%,满足试验要求。                                          2018,40(4):357-360.
                  本工作采用特制毛细管色谱柱结合GC-MS快                              JIN  D  Q,DING  B  D,GONG  A  Q,et  al.  HPLC
              速测定水中6种有机磷农药的残留量。该方法快速、                                determination of sethoxydim and dicamba in vegetables
              准确,能有效降低成本,满足DB 31/199—2018《污                          with  accelerated  solvent  extraction[J]. Chemical
                                                                     Reagents,2018,40(4):357-360.
              水综合排放标准》、GB 3097—1997《海水水质标准》、
                                                                 [7]   陈彩霞,王长华,周海收,等. GC-MS在环境保护领域
              GB/T 14848—2017《地下水质量标准》等标准中目
                                                                     的应用[J]. 光谱实验室,2013,30(6):2901-2905.
              标物的检出限要求,适用于大批量水体样品中有机                                 CHEN  C  X,WANG  C  H,ZHOU  H  S,et  al.
              磷农药的测定。                                                Application  of  gas  chromatography-mass  spectrometry
                                                                     technology  in  environmental  protection[J]. Chinese
              参考文献:
                                                                     Journal of Spectroscopy Laboratory,2013,30(6):2901-
               [1]   李湄琳. 农药残留及其对环境的污染[J]. 环境与发展,                    2905.
                   2017,29(9):56-56.                             [8]   余蕾,张小毅. 气相色谱-三重四极杆质谱法测定地
                   LI  M  L.  Pesticide  residues  and  their  environmental   下水中44种有机物污染物[J]. 岩矿测试,2021,40(3):
                   pollution[J]. Environment  and  Development,2017,   365-374.
                   29(9):56-56.                                      YU  L,ZHANG  X  Y.  Determination  of  44  organic
               [2]   王伟力,林彩,刘洋,等. 钦州湾沉积物中重金属的多                       pollutants  in  groundwater  by  gas  chromatography-triple
                   元统计分析:空间关系、生态风险和来源识别[J]. 应用                       quadrupole  mass  spectrometry[J]. Rock  and  Mineral
                   海洋学学报,2024,43(1):135-146.                         Analysis,2021,40(3):365-374.
                   WANG  W  L,LIN  C,LIU  Y,et  al.  Multivariate    [9]   陈绍华,郑清林. 全自动固相萃取-气相色谱-三重四
                   statistical  analysis  of  heavy  metals  in  sediments  of   极杆串联质谱法测定地下水中甲基对硫磷[J]. 分析仪
                   Qinzhou  Bay:Spatial  relationship,ecological  risk   器,2023(3):40-44.
                   and  source  identification[J]. Journal  of  Applied       CHEN  S  H,ZHENG  Q  L.  Determination  of  methyl
                                                                     parathion  in  groundwater  by  automatic  SPE  and  GC-
                   Oceanography,2024,43(1):135-146.
               [3]   刘雪梅,孙洪. 山东济宁肥料管理与土壤改良技术[J].                     MS/MS[J]. Analytical Instrumentation,2023(3):40-44.
                   农业工程技术,2023,43(27):24-25.                     [10]  谢沙,胡英辉,秦迪岚,等. GC-MS测定地表水中28种
                   LIU  X  M,SUN  H.  Fertilizer  management  and  soil   有机磷农药[J]. 山东化工,2024,53(14):180-185.
                   improvement  technology  in  Jining,Shandong  Province       XIE  S,HU  Y  H,QIN  D  L,et  al.  Determination  of
                   [J]. Agricultural Engineering Technology,2023,43(27):  28 organophosphorus pesticides in surface water by GC-
                   24-25.                                            MS[J]. Shandong  Chemical  Industry,2024,53(14):
               [4]   樊吉平. ECD-气相色谱法同时测定多种有机氯和有                       180-185.
                   机磷农药[J]. 中国卫生检验杂志,2012,22(6):1253-            [11]  关小桃,张琪雨,黄军如,等. 高效液相色谱-串联质谱
                   1254.                                             法直接进样快速测定水中的27种农药[J]. 广东化工,
                   FAN  J  P.  Determination  of  organochlorine  and   2021,48(11):144-146.
                   organophosphorus  pesticides  by  ECD-GC[J]. Chinese       GUAN  X  T,ZHANG  Q  Y,HUANG  J  R,et  al.
                   Journal of Health Laboratory Technology,2012,22(6):  Rapid  determination  of  27  pesticides  in  water  by  high
                   1253-1254.                                        performance  liquid  chromatography-tandem  mass
               [5]   郑远利,马莉莉,吴晓波,等. 固相萃取-高效液相色谱                      spectrometry  with  direct  injection[J]. Guangdong
                   法测定水中3种有机磷农药残留[J]. 理化检验-化学分                       Chemical Industry,2021,48(11):144-146.
                   册,2017,53(3):355-358.                         [12]  余璐,宋伟,吕亚宁,等. 超高效液相色谱-四极杆-飞
                   ZHENG Y L,MA L L,WU X B,et al. Determination      行时间质谱法快速筛查茶叶中的204种农药残留[J]. 色
                   of  three  organophosphorus  pesticide  residues  in  water   谱,2015,33(6):597-612.
                   by  solid  phase  extraction-high  performance  liquid       YU L,SONG W,LÜ Y N,et al. Rapid determination
                   chromatography[J]. Physical  Testing  and  Chemical   of  204  pesticide  residues  in  tea  by  ultra  performance
                   Analysis Part B:Chemical Analysis,2017,53(3):355-358.  liquid  chromatography  coupled  with  quadrupole-time
               [6]   金党琴,丁邦东,龚爱琴,等. 快速溶剂萃取高效液相                       of  flight  mass  spectrometry[J]. Chinese  Journal  of
                   色谱法测定蔬菜中烯禾啶和麦草畏残留[J]. 化学试剂,                       Chromatography,2015,33(6):597-612.



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